Sinteza MDMA iz piperonilmetilketona (PMK/MDP2P) z mravljično kislino

Followme38

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Ali lahko namesto nmf uporabite standardni formamid ?
 

CryoThio

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Pri tem boste izdelali MDA in ne MDMA, vendar da, lahko. Metilna skupina je potrebna za nastanek mdma
 

Jasonmorales77

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Ali bi lahko ustvaril MDA s tem načinom spreminjanja česa, ali mi lahko kdo razloži, kako?
 

CryoThio

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Na tem mestu bi moralo biti na voljo nekaj zapisov.

Mda nastane z reakcijo formamida z mdp2p.

Mdma nastane z reakcijo n-metilformamida z mdp2p.
 

Camilo

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Ali bi to delovalo za sintezo MDA iz M.Dfenilacetona?
 

blitzen.maniax

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Če uporabljate izomer S za MDMA, vas opozarjamo, da če se namesto tega odločite za izdelek MDA, potem potrebujete izomer R za MDA in S za MDMA . Dobra stvar je, da če to pravilno načrtujete, ni odpadkov
 

bitcoinup2020

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Pozdravljeni, sem začetnik.

Rad bi vprašal o temi 4.
4. Tej raztopini dodamo koncentrirano klorovodikovo kislino (HCl 36 % 30 ml). Nato reakcijsko zmes segrevamo pri 80 °C še 3 ure.

Ali lahko namesto klorovodikove kisline 36 % uporabim klorovodikovo kislino 35 %?
 

2-79-790125

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bitcoinup2020
Nikoli nisem uspešno izdelal MDMA, vendar v mojih raziskavah HCl 35% proti HCl 36% nima nobene pomembne razlike za katero koli sintezo MDMA. Imamo srečo, da ne zahteva tako natančnih toleranc. Da bi bilo jasno, sem popoln Rookie z omejenimi izkušnjami in to je moje mnenje.
 

ZACARIASKLK123

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Skupno 7,32 g, ki se doda kot celota v enem koraku?
ali
7,32 g mravljinčne kisline, dodajanje razdeljeno v 7 urah z uporabo kapalnega lijaka?
 
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The FALCON

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Mdp2p mora biti najprej olje ali prah ?če olje, kako pretvoriti prah v olje ?
 

The FALCON

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S čim lahko nadomestim plin hcl?
 

hider8028

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Ali je olje MDP2P pravo? Kako je z 9Gram?
 

Tegridy

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koliko časa bi v povprečju trajal ta postopek?
 

WillD

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Ta postopek lahko razdelimo na dve fazi (in dva dni), pri čemer rezultat dobimo tretji dan. Lahko pa ga tudi količinsko razširite. Objavljeno sintezo bomo v prihodnosti uredili, da bi povečali produktivnost (uporaba dodatne vode v reakciji).
 

mickael1985

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Pozdravljeni
Kakšne količine acetona in kloridne kisline je treba dodati k olju MDMA Freebase Oil? Kako potem izločiti kislino in aceton? Nisem kemik, hvala, ker ste mi to posledično razložili.
 

WillD

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5:1 aceton:aq.hcl~37% pri min. Po kristalizaciji v zamrzovalniku vsaj en dan, če nimate izkušenj. Po filtraciji pustite usedlino in nadaljujte s kristalizacijo.
 

ImRegistered

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Ali lahko mravljinčno kislino nadomestimo? Hipofosfor?
HCl, dodana raztopini N-formil-MDMA, kakšen Ph mora imeti?
Ali kdo ve, kakšen je izkoristek?
 
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Win Win

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Pišete PMK pomeni, ali lahko neposredno uporabite PMK v prahu za to?
 

Alojz

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Ustvarite lahko videoposnetek sinteze PMK in MDMA
 

The goal

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Pozdravljeni vsi, rad bi vas nekaj vprašal o nečem, pri sintezi mdma, kakšne so alternative di-etil etru? ali lahko uporabim toluen ali dcm?, tudi o plinu hcl, ali lahko uporabim tekočino hcl z acetonom ali žveplovo kislino? tudi o količini mgso4, hvala.
 

The goal

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V številki 4, koliko hcl je potrebno za 3L olja ?
 
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