Syntéza JWH-018. Malý rozsah.

Bigwest

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Mám všetky zložky, snažím sa Rozdeliť 8 a 4 minúty ožarovania na 2 po 2 minúty a nechať thé produkt medzi nimi vychladnúť, ale nefunguje to. Mohol by mi s tým niekto pomôcť pls.
 

G.Patton

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Môžete sa pokúsiť rozdeliť ho na 10 až 25 sekúnd. Neochladzujte ich príliš.
 
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Bigwest

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Ahoj
Skontroloval som všetky body topenia mojich surovín. Evry thing its OK. Vyskúšali ste túto syntézu pomocou domácej mikrovlnnej rúry ?

Myslím, že to nebude fungovať. môže sa to urobiť len pomocou mw reaktora.
 

G.Patton

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Ahoj, ja som to neurobil. Na túto syntézu som sa pýtala za vás od Williama. Ty za tvoju spätnú väzbu.
 

Bigwest

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Píšem williamovi v pm. Dúfam, že hé odpovie. Ale som sûre, že Theres niečo nie je v poriadku.
 

Nicky

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Dobrý deň. Len malé vysvetlenie prosby.
Ako dlho by sme mali ožarovať výrobok pri použití domácej mikrovlnnej rúry---8--4 minúty alebo 10---25-- sekúnd? A musí byť šálka uzavretá?
 

Nicky

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Používame 400 W aj v domácej mikrovlnnej rúre ?
 

41Dxflatline

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Ak fungujú mikrovlny, mal by fungovať aj ultrazvuk
 

Alex7920

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Aký typ mikrovlnnej rúry je vhodný na túto reakciu? Môže sa táto reakcia uskutočniť pomocou domácej mikrovlnnej rúry?
 

joejoe354354

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Dobrý deň,chcel by som sa opýtať, či je táto metóda nof vhodná na hromadnú výrobu?
 

HerrHaber

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To môže byť možné len s pomocou prietokového typu MW reaktora, ktorý možno poňať ako improvizovaný z domáceho zariadenia, ale potrebuje niekoho s pomerne veľkými skúsenosťami a guľami.
 

pakanahesa

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Dobrý deň, bratia, pozdravujem vás majster. Jeho malá mierka pre ľahkú dávku alebo silnú dávku? Thx. Coz som to vyskúšal 1. jeho účinok nie je vôbec
 

William D.

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2-3 mg na jeden zásah. u môže reakciu uskutočniť vo fázach, ktoré kontrolujú úspešnosť každej fázy.
 

robloxgelap

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all the ingredients are easily available, but making it looks difficult. is there anyone who can help me? especially for steps 6, 7, and 8 how to filter aluminum oxide, what is the temperature for reflux, and what is the aluminum oxide filtered and then washed for? because in the next step aluminum oxide is not mentioned that it will be used again.
 

soebunies

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@robloxgelap aluminium oksida ga larut dalam etanol, suhu reflux adalah suhu titik didih pelarut, tujuan pencucian aluminium oksida agar bisa digunakan kembali di reaksi berikutnya
 
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robloxgelap

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berarti untuk membuat kembali jwh, ga perlu beli alumunium oksida lagi? dan bisa pake alumunium oksida yang sebelumnya udah pernah dipakai dan sudah di cuci?
 

soebunies

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benar, hati hati sama asep kuning yang keluar, harus selalu dipantau ya👍
 

pakanahesa

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Cek pm bro, anyway ane pake microwave rumahan itu waktu dan suhunya tetap 100 celsius atau waktunya lebih lama bro. Soalnya ga ngefek bro
 

mycelium

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I don't understand people not being able to hear EtOH in the microwave
Or maybe around here everyone has cannabis oil and makes candy and shit.
Microwaves have lights inside.
With 50ml ethanol, I hear it for 15 seconds which is normally enough to make it real warm.
Then short bursts, and looking at the beaker in the microwave.
The slightest bubbles and you stop , because it goes from a couple bubbles to over boiling almost instant.
 

William D.

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Yes, you are right. It is often necessary to stop heating, it will be gradual. But there is a solution that looks like this:
P9LmxJuQFb

The condenser is installed through the seal.
 
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