Question, how is it that the MDA freebase mixes with the petroleum ether added after distillation but after the aluminum oxide addition and filtering, the petroleum ether added before HCl gassing does not mix with the MDA freebase petroleum ether mixture that was filtered?
Question, how is it that the MDA freebase mixes with the petroleum ether added after distillation but after the aluminum oxide addition and filtering, the petroleum ether added before HCl gassing does not mix with the MDA freebase petroleum ether mixture that was filtered?
As someone who done it many times I can tell you one thing, you can purify your product much easier and actually get perfectly white, sparkly amine.
What you do is dissolve crude amine in small amount of boiling EtOH (4-5ml per 1g), after full dissolution add at least 5 times the volume of anhydrous acetone, put in a fridge for a few hours, filter and wash with acetone. That’s it
Your method is a simple recrystallization from a solvent. Of course, it is easier and gives results. The video shows classic acid-base extraction, which has much better qualities for purifying substances. This method can be used for many amphetamine group compounds, such as amphetamine, meth, MDMA, TMA, 2c-b, etc.
As someone who done it many times I can tell you one thing, you can purify your product much easier and actually get perfectly white, sparkly amine.
What you do is dissolve crude amine in small amount of boiling EtOH (4-5ml per 1g), after full dissolution add at least 5 times the volume of anhydrous acetone, put in a fridge for a few hours, filter and wash with acetone. That’s it
The production values on these videos keeps getting better! This video is so perfectly panned, focused, lighted, synced, transitioned, soundtracked.....It looks like a million dollars. i can also appreciate that you've stuffed every scene with visual information instead of dialog. It makesmyounwonder and think instead of just being a verbatim step-by-step routine to follow
As someone who done it many times I can tell you one thing, you can purify your product much easier and actually get perfectly white, sparkly amine.
What you do is dissolve crude amine in small amount of boiling EtOH (4-5ml per 1g), after full dissolution add at least 5 times the volume of anhydrous acetone, put in a fridge for a few hours, filter and wash with acetone. That’s it
As someone who done it many times I can tell you one thing, you can purify your product much easier and actually get perfectly white, sparkly amine.
What you do is dissolve crude amine in small amount of boiling EtOH (4-5ml per 1g), after full dissolution add at least 5 times the volume of anhydrous acetone, put in a fridge for a few hours, filter and wash with acetone. That’s it
Really appreciate all the work that went into these videos. But I’m curious about the solvent recrystallization. Using the results from the previous video. How exactly would you go about recrystallizing the 100g mad.hcl? For the 100 g of mda.hcl you would need 4000ml etoh and 20,000ml(for 5 times volume) of acetone? Does that not seem like a lot of acetone What would the yield on the 100g mda.hcl be?
Really appreciate all the work that went into these videos. But I’m curious about the solvent recrystallization. Using the results from the previous video. How exactly would you go about recrystallizing the 100g mad.hcl? For the 100 g of mda.hcl you would need 4000ml etoh and 20,000ml(for 5 times volume) of acetone? Does that not seem like a lot of acetone What would the yield on the 100g mda.hcl be?
Bro, it's wrong calculation that you done
For 100g MDA.HCL, need 400 to 500ml etoh(for 1g mda hcl, 4 to 5ml etoh)
And 5times of aceton that would be 2000ml to 2500ml
I hope it helps to you
Bro, it's wrong calculation that you done
For 100g MDA.HCL, need 400 to 500ml etoh(for 1g mda hcl, 4 to 5ml etoh)
And 5times of aceton that would be 2000ml to 2500ml
I hope it helps to you
Thanks man. Appreciate the response. Shortly after posting that I realized I fucked up my simple math! Also read G.Pattons post about solvent purification and it answered a lot of questions. One that I still am unaware of.. What sort or yield should you expect from 100g mad.hcl with this method?
