P2P synthesis from BMK glycidate ethers

[merlin]

It would be good if we had one like this pmk to mdma

 

[adbb5clsupplier]

sure,cas 28578-16-7

 

[Jesse_Pinkman_]

Here:

A Photo Essay on the Nitromethane Al/Hg

 

[G.Patton]

Hello, can you ask more clearly please? Do you want to convert PMK glycidate to MDP2P and than to MDMA? There is method on our forum how to get MDP2P. MDP2P -> MDMA. Look around Amphetamines forum section.
Synthesis of MDMA from piperonylmethylketone (PMK) with formamide and LAH
Synthesis of MDMA via Pt/H2 (small scale)

Hello, you can advice our forum topics with better explanation as well. I would be very appreciated. There is method with pictures Complete MDMA synthesis from sassafras oil. There are photos of stages from MDP2P to MDMA and detailed explanation.

 

[Mr.Blanks00]

Sir, I want to ask, how do we test that the reagents we make are p2p correct.

 

[G.Patton]

First of all, you can cheek general appearance and than measure boiling point.

 

[heliosyang]

Is the starting material [cas 41232-97-7] or [cas 80532-66-7]?

 

[G.Patton]

Hello, you can use both of them as precursor.

 

[diogenes]

Can anyone advice on which precursor is best to buy I mean safest to ship to Europe? Is any of the BMK powders legal - where can this be checked? I`m a bit confused as there are quite a few versions available.

 

[adbb5clsupplier]

BMK5449-12-7

 

[KokosDreams]

P2NP is legal
P2P is restricted
BMK Glycidate 5449 is still quite new and as far as I know not restricted, altho it is common knowledge what glycidates are used for, especially bmk glycidates.

My guess would be that P2NP is the safest bet

 

[Saul]

1-Phenyl-2-nitropropene, or simply phenyl-2-nitropropene, or P2NP, as it is commonly ... amphetamine class, and are listed as drug precursors in many countries

Phenyl-2-nitropropene - Wikipedia

en.wikipedia.org

Bmk salt cas 5449-12-7 is still verry new in de scene it is worldwide allowd and till today not listed in no country.

also prices off P2NP go with the wind I mean not stable prices . the bmk salt is sent from europe with secure shipping line
it cost something like 100€ / kg

 

[KokosDreams]

P2NP is not restricted so far in most of the countries.

 

[Saul]

I copy paste from pedia

 

[KokosDreams]

Yeah the Wikipedia article is actually a little wrong. There are much more usecases for P2NP and it's not restricted

 

[caesare.robot]

SWIM started with [cas 5449-12-7] after 4h of heating got aqueous layer on top and oily bottom... what did wrong? too much acid?

 

[caesare.robot]

further attempts with cas 5449-12-7 and step 1 of described method gave proper and stable results!

 

[Bartholomeus]

Please post some pictures, there should be no problem i think

 

[Saul]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/p2p-synthesis-from-bmk-glycidate-ethers.4307/post-13418

 

[caesare.robot]

as far SWIM understands the P2P oily layer should float after reflux and heating? (temperature was constant 90°C. PH1.)

 

[blackburn]

You have some pictures?

 

[G.Patton]

Phenylacetone (P2P) has Density: 1.0057 g/cm3; Hence - your layer heavier than water. It means that it have to be on a bottom. Vice versa, if your water layer is heavier by reason of dissolved salts, p2p layer will be on a top. What is a problem to check boiling point?

 

[h20]

This is a very interesting question.
If we cook BMK salts, then the top layer is the p2p
if we now pour this top layer into a measuring cup, and we add warm water. Then the water is the top layer.