Nicely done.
so if you were to want to make MDMA via this route would you be forced to go through MDA and then methylate?
not something I’m looking to do, just interested.
Nicely done.
so if you were to want to make MDMA via this route would you be forced to go through MDA and then methylate?
not something I’m looking to do, just interested.
Hello, which hydrate of Na2CO3 is implied here?
And how many mEq of helional are used? Amount seen in beaker does not match the mount stated in text.
Just trying to figure out molar ratios
Hello, which hydrate of Na2CO3 is implied here?
And how many mEq of helional are used? Amount seen in beaker does not match the mount stated in text.
Just trying to figure out molar ratios
By reductive amination reaction between mdp2p and methylamine just like p2p to meth, its easy but How did you get mdp2p? Are you sure a bout what you recived is mdp2p specially from naserkhosro sellers? Idoubt you synthesis mdp2p by your self .
By reductive amination reaction between mdp2p and methylamine just like p2p to meth, its easy but How did you get mdp2p? Are you sure a bout what you recived is mdp2p specially from naserkhosro sellers? Idoubt you synthesis mdp2p by your self .
I reached the final product, but if you weren't so inexperienced, you would understand that the P2P conversion method isn't suitable for MDP2P. Also, if you lack the ability to discern, that's your problem; not everyone is like you. I just want to see how this journey unfolds with the skilled hands of someone like Navator. Moreover, Tehran is not just Nasser Khosrow; keep yourself updated.
By reductive amination reaction between mdp2p and methylamine just like p2p to meth, its easy but How did you get mdp2p? Are you sure a bout what you recived is mdp2p specially from naserkhosro sellers? Idoubt you synthesis mdp2p by your self .
اولا من به محصول نهایی خیلی وقته رسیدم دوما اگه مبتدی نبودی و حداقل 1 بار امتحان کرده بودی میدونستی مسیر پی دو پی مناسب مسیر ام دی پی دو پی نیست
از پشت گوشی با دیدن 4 تا ویدئو بگی لنگش کن خیلی راحته و اینکه بگی راحته خودش اثباته مبتدی بودنته شیمی هیچوقت 100درصد نیست
بعدشم خودت رو آپدیت کن تهران تو ناصر خسرو خلاصه نشده
و تمرین کن شاید ام دی پی دو پی رو یه روز تونستی تشخیص بدی
برای من راحته
Lolll. Congrats about your results . Ok you are professional and im just copy writer . I never show my results on internet and understand that you are has no ability to analyse the rules but no problem atleast watch out for dogs. Yes there are a lots of ways to turn isosafrole to mdma like performic acid oxidation to mdp2p. Im not here to defend my self as an exprienced chemist and there is no price in it for me.The best way is the way that you can get reagents easy and without suspicious .
Best regards
I reached the final product, but if you weren't so inexperienced, you would understand that the P2P conversion method isn't suitable for MDP2P. Also, if you lack the ability to discern, that's your problem; not everyone is like you. I just want to see how this journey unfolds with the skilled hands of someone like Navator. Moreover, Tehran is not just Nasser Khosrow; keep yourself
You mean from helional? I’m more interested in the theory of getting from melional to MDMA - it’s not something I am likely to do but it’s interesting.
I know there are easier ways to get to mdma
I make already the mda nice , but i got problem to make mda to mdma i follow this way but i lost all my mda.
179 g (1 mole) of MDA as the free base and 106 g (1 mole) of benzaldehyde are dissolved in 95% ethanol (as much it takes to dissolve them). This solution is refluxed for 30 minutes forming the Shiff base (imine) intermediate of these two compounds. The ethanol is removed by distilling under reduced pressure leaving an oil.
This oil is added to 142 g (1 mole) of methyl iodide and placed in a pipe "bomb". Use a pipe with fine threads and wrap these with teflon tape to form a good seal. Tighten down the caps well and place the pipe "bomb" in boiling water for five hours. The material in the "bomb" is then washed out with a solution of 80ml methanol and 10 ml water and placed in a boiling flask to be refluxed. Only enough solution to rinse out the pipe is required. Reflux the mixture for 30 minutes. Add an equal volume of water and reflux the mixture until the odor of benzaldehyde has disappeared. Acidify the mixture with hydrochloric acid (shake well) and the extract with three portions of ether. The solution is made basic with 25% NaOH solution and the liberated amine is extracted with ether (or methylene chloride etc.). The ether is washed with water, dried with MgSO4 and HCl gas is run into the solution to precipitate the amine. Filter and allow to dry.
The MDMA may contain some MDA but this should be acceptable. Replacing methyl iodide with 156g (1 mole) ethyl iodide and boiling the pipe for 10-15 hours will give Eve.
From hier i got the problem Add an equal volume of water and reflux the mixture until the odor of benzaldehyde has disappeared. Acidify the mixture with hydrochloric acid (shake well) and the extract with three portions of ether. The solution is made basic with 25% NaOH solution and the liberated amine is extracted with ether (or methylene chloride etc.).
I do not think that is the case. The solution foams with the relaease of free hydroxlamine similar to the video, and the materials are high quality. Could it be that room temp is too cold at 15 C. Should I try applying slight heat?
I do not think that is the case. The solution foams with the relaease of free hydroxlamine similar to the video, and the materials are high quality. Could it be that room temp is too cold at 15 C. Should I try applying slight heat?
It is oiling out instead of crystalyzing. I don't know how to get it to crystalyze. I understand that this probably means an incomplete reaction/impure products. But I think it is mostly Oxime. The oil is easily seperated from the water layer. Do you think it can be treated in some way to get it to crystalize? I found this and I belive the same thing is happening with me.:
It is oiling out instead of crystalyzing. I don't know how to get it to crystalyze. I understand that this probably means an incomplete reaction/impure products. But I think it is mostly Oxime. The oil is easily seperated from the water layer. Do you think it can be treated in some way to get it to crystalize? I found this and I belive the same thing is happening with me.:
No idea if this is relevant because I havnt run this reaction but some oils that form instead of crashing out crystals is due to impurities and can be re-crystallised as you would crude solid material.
As I say, no idea if it’s the case for this though…
good luck
It is oiling out instead of crystalyzing. I don't know how to get it to crystalyze. I understand that this probably means an incomplete reaction/impure products. But I think it is mostly Oxime. The oil is easily seperated from the water layer. Do you think it can be treated in some way to get it to crystalize? I found this and I belive the same thing is happening with me.:
don't worry and don't panic
helional oxime can be in oil form - this is normal
if you want the crystals (but why?) - rubbing the oil with using glass rod , maybe it crystallized
confirmation that this is oxim will be a conversion reaction into amide
don't worry and don't panic
helional oxime can be in oil form - this is normal
if you want the crystals (but why?) - rubbing the oil with using glass rod , maybe it crystallized
confirmation that this is oxim will be a conversion reaction into amide
Wow thank you. I did not panic, and I patiently let it settle for a little over a day, and it magically solidified into a beautiful paste. I am still not sure why mine did not crystalize in solution like the video. And nor do I know what led it to crystalize other than time. What do you think was preventing it from solidifying the whole time? Nonetheless, I am satisfied. On to the next step!
Wow thank you. I did not panic, and I patiently let it settle for a little over a day, and it magically solidified into a beautiful paste. I am still not sure why mine did not crystalize in solution like the video. And nor do I know what led it to crystalize other than time. What do you think was preventing it from solidifying the whole time? Nonetheless, I am satisfied. On to the next step!
