La mia sintesi di 3-CMC

[mithyl2]

è fantastico.

perché pensi che il congelatore ti abbia dato risultati strani durante la cristallizzazione?

Quanto pensi che questo metodo sia scalabile?

 

[Jesse_Pinkman_]

A causa dell'acqua, quando si congela, da dove dovrebbero provenire i cristalli?
Il normale frigorifero forse funziona, ma ho il mio cibo all'interno e non voglio pulirlo ogni volta.
Ho provato davvero molti modi per arrivare al prodotto finale e ho anche sprecato molti solventi e 2b3c, ma il modo in cui ho descritto ha funzionato meglio degli altri tentativi.
Mi sono quasi confuso con tutti i metodi diversi, tutte quelle ciotoline con miscele diverse erano in giro, ho sempre guardato quale si sviluppava bene e quale no.
Per esempio, quando si mette l'ipa ghiacciata nell'acqua/polvere di cristallizzazione, si ottengono immediatamente dei cristalli bianchi, ma non sono chiari e sono solo un po', quindi bisogna cristallizzare di nuovo e il resto deve evaporare, guarda l'ultima foto.
Le altre 3 foto mostrano cosa succede alla rm nel mio freezer, diventa una massa solida che si scioglie a temperatura ambiente, ma senza cristalli.

 

[HerrHaber]

it depends on how much material you want to dissolve and the water to alcohol ratio.

 

[HardWork]

Is it possible to make 3mmc in powder ? Everyone is talking about acidification with water or acetone and then straight to dish and evaporate. But maybe it is possible to make it like 4mmc. Just putting HcL straight to washed rm and powder forming. Is it possible with 3cmc ? And how to do it with dcm ?

 

[SunDay]

I dont want to disapoint you, but no... how much i know ( i read all topics about 3cmc). Just evaporation way

 

[SunDay]

But its strange, becouse everythime when i wash stuff with acetone I put acetone to fridge, and after some time i get 3cmc powder. why its not happening when acidifying with acetone from begining..?

 

[HardWork]

I have tried reaction with toluen,and then tried to put only HCL,so I’ve got some powder. But yield was only 25%

 

[SunDay]

I tried this also. 1st time my HCL was 80% (it perfectly fits for H2O acidification in proper amount) but when only HCL, everything BURNT ), and second time with 26-38% so drop was sticky flufy mass(then you need MUCH work to get crystals from this shit, and yeld was about 35%.
By the way, in market there is 28% HCL, it comes from latvia.. that shity HCL makes problem with acidification, purple or emerald color goes on, and really hard to achieve optimal ph. All latvian chem in shops ar shit, so dont be fooled.

 

[HardWork]

Yeah,I have used 26-38% hcl and get 25% yeld.

 

[Jesse_Pinkman_]

Same, always had 25-30% after several washing and recrys...there are methods with more yield for sure, but my experiences were always around this amount

 

[EL Mayo]

Then u how made u get only 30% haha I get minimum 60% i wait week and get crystal if i need powder easy get out in freezer form dark Orange oil all water take out

 

[EL Mayo]

.