UR-144 synthesis from TMCP-indole (large scale). Complete video tutorial.

MrSung

Don't buy from me
Resident
Joined
Mar 23, 2022
Messages
61
Reaction score
18
Points
8
Good, thanks for your response
 

hgfhgjkh

Don't buy from me
New Member
Joined
Dec 23, 2021
Messages
10
Reaction score
7
Points
3
@HIGGS BOSSON, can you tell me what was the final yield in your video? Thanks
 

WillD

Expert
Joined
Jul 19, 2021
Messages
774
Reaction score
1,054
Points
93
Yield is written in the article, but for different intermediates will be slightly different.
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
52
Reaction score
13
Points
8
where i get TMCP-indole ? anyone got already?
 
Joined
Jul 25, 2021
Messages
194
Reaction score
306
Points
63
TMCP-indole is made to order or by yourself. You need to find a chemist who will agree to synthesize it for you, or use the services of a company that does custom syntheses. If you decide to make it yourself, you should contact our Experts. The method of synthesis is written here.
 
Last edited by a moderator:

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
52
Reaction score
13
Points
8

can you tell me a company which does custom synthesis?
and where i can order the integridents for the TMCP-indole synthesis?
please i need someone tell me trusted sources,
i am completely new in learning working with synthesis.
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
52
Reaction score
13
Points
8
I am glad that i have found this forum.
Where it was hidden all the time,
that i not know of its existence, until few weeks ago ^^
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
52
Reaction score
13
Points
8

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
52
Reaction score
13
Points
8
and CH2Cl2 from india`? or can i use also Dichloromethane Anhydrous from an european vendor, like nitromethane?

the other integridents i not found yet. SnCl4 and 2,2,3,3-Tetramethylcyclopropanecarbonyl chloride.
 

abbadon

Don't buy from me
Resident
Language
🇺🇸
Joined
May 4, 2022
Messages
52
Reaction score
13
Points
8

aaronstevens

Don't buy from me
Resident
Joined
Mar 18, 2022
Messages
67
Reaction score
126
Points
33
Deals
16
Does anyone know where I can buy these raw synthetic cannabinoids such as jwh-018 and ur-144
 

BoonDock

Don't buy from me
Resident
Joined
Jul 29, 2022
Messages
33
Reaction score
12
Points
8
The video shows a wash at the end using alcohol and a heating up process. The instructions with the pictures do not have this. Whats the best thing to do once you take off the top layer and put it in a mold?
 

BoonDock

Don't buy from me
Resident
Joined
Jul 29, 2022
Messages
33
Reaction score
12
Points
8

dnkr

Don't buy from me
New Member
Joined
Aug 11, 2022
Messages
19
Reaction score
7
Points
3
I swear UR-144 was the next best thing after JWH-018.. not crazy strong with risk of detrimental effects but I remember very high quality and smooth research experience

If someone can help me find trusted supplier for main precursor I would greatly appreciate it . i would rather make my own then not know what i'm getting these days
 

khundongdong

Don't buy from me
New Member
Joined
Feb 21, 2022
Messages
17
Reaction score
4
Points
3
is this the cas number for the first item?
895152-66-6
 

WillD

Expert
Joined
Jul 19, 2021
Messages
774
Reaction score
1,054
Points
93
yes
Write to Zero Day, perhaps he will help.
If everything was done correctly, wait until it hardens.
For raw materials for synthesis, use listing or write to Zero Day.
 

dnkr

Don't buy from me
New Member
Joined
Aug 11, 2022
Messages
19
Reaction score
7
Points
3

Can you elaborate more on this step? Specifically the "ice alcohol". Does the isopropyl alcohol need to be cooled to a specific temp before pouring to wash? (and does it need to be 99% or would 70% work)?

Also, I'm just curious why the post pictures and your video the top layer to collect with syringe is different colors (the video is dark yellow and yours is more of a dark red? Is that normal? (For my first time synth I don't want to think I messed up if mine turns a completely different color lol)

And I want to thank you very much for the video! I hope we can see more from you for other cannabinoid synths
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,704
Solutions
3
Reaction score
2,845
Points
113
Deals
1
Yes, you have to cool it in freezer. In opposite case your product will dissolved partially in warm IPA. Same with 70% IPA. It has to be dry and 99% concentrated.
 

Zachargi

Don't buy from me
New Member
Joined
Aug 28, 2022
Messages
1
Reaction score
0
Points
1
Can I replace 1-Bromopentane with 1-bromobutane?
 
Top