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Aluminium amalgam (Al/Hg) Summary
Kan dette bruges til at erstatte synteser, der kræver NaBH4? Jeg prøver at lave 5-MeO-DMT ud fra 5-MeO-T efter Hamilton Norris' syntese, men jeg har ikke NaBH4 til rådighed.
- By G.Patton
Det tror jeg ikke
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Er der en måde at fremstille NaBH4 på, som ikke kræver superhøje temperaturer eller tryk, og som kan udføres i lille skala i et amatørlaboratorium, eller skal jeg bare give op og bestille fra Kina og håbe, at tolden ikke stiller spørgsmålstegn ved mig?
Hvorfor virker Al/Hg ikke til den syntese? Det burde reducere iminen til methylering af tryptaminet, ikke?
Jeg tror, det kan lade sig gøre, men jeg er ikke helt sikker. Tror du, at det vil reducere dobbeltbindingen på indolen?
Den eneste ting, jeg ikke er helt sikker på, er produktet, vil det lave MMT eller DMT. I din syntese af metamfetamin fra amfetamin med Al/Hg tilføjes der kun en methylgruppe til aminen.
Når man har lavet en opløsning af kviksølv i salpetersyre og derefter tilsat denne opløsning til en kolbe med vand og aluminiumsfolie, hvordan udlufter man så dampene fra denne reaktion korrekt? Dampene virker stærke nok til, at de slipper ud af luftfilteret og også går gennem masken. Jeg tænkte på at bruge vakuumpumpen med kolben og derefter en vakuumregulator, så vakuumstyrken er lige nok til, at dampene kan udluftes udenfor, men jeg er bekymret for at pumpe brintgas, da det kan risikere at eksplodere.
Hej, kan jeg bruge den samme mængde kviksølv (Ii) chlorid som kviksølv (Ii) nitrat til syntese af amfetamin pls
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
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A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol