Jag försöker 4mmc?

[Toddler]

plz check the whole process and plz tell me which step i do mistake, mixture not perform white Flappy liquid.


20g 2b4m
100ml EA
stirrer until dissolve,
Then add 40ml MA 40%.

stirrer 1 hours temp not goes above 30.2. Without water bath.

then put in separating funnel.
first wash once with bicarbonate 5% 60 ml solution,

then 3 time wash with cold water 60ml x 3 times

After wash add 200ml chilled acetone.
Then dropping add hcl 33%.

After some add hcl color change yellow to brown.
Then

after some drop like 3-4 drop add hcl
change brown to green

after some time without dropping hcl color change to yellow.
But not performing white liquid.
As all saying

 

[Toddler]

@William D. @Dr. MMX


I cooked one more batch.

150g 2b4m
600ml EA

300ml 40% MA aq. ( take 10min gap every after 50ml add 6x50ml)

after that left stirrer 2 hours temp range 20-30 using ice batch

(should this be done this way)

added 5% sodium bicarbonate once with 450ml water

and after that washed 450ml water x 3 times.

kept it in fridge for 8 hours at 1• degree temp.

after that add acetone 800ml within mixture -18 degree

stirrer 5 min mixture temp -10 degree.

then add HBR 48% 50ml drop wise until ph become ph5.

I have found what is in the image.

In this small crystals are made of small like needles

 

[dodobird]

So far it looks great bro..congratulations...

What did you do once you reached the above image?

Fridge 8 to 10 hours?