- Language
- 🇫🇷
- Joined
- Apr 10, 2022
- Messages
- 300
- Reaction score
- 170
- Points
- 43
Hi guys...
So... I have try with what i have in stock.
Fiiiiiirst try, totally noob
To 55 g (0.5mol) Benzaldehyde in a 500mL Flask were added 40 g (0.5mol) Nitroethane and 10mL Cyclohexylamine. All was refluxed for 6h on a water bath. The result were 2 layers.
after that, cooling at room temperature...
after, 50mL of H2O were added and then sucked off with a pipette, 4 times.... but nothing happens, except reforming of 2 layers... (no photo sorry)
after, i have separate the 2 layers, and put 50ml of isopropanol in the orange one
and i put it in the freezer... (actually 11h)
to be continued...
So... I have try with what i have in stock.
Fiiiiiirst try, totally noob
To 55 g (0.5mol) Benzaldehyde in a 500mL Flask were added 40 g (0.5mol) Nitroethane and 10mL Cyclohexylamine. All was refluxed for 6h on a water bath. The result were 2 layers.
after that, cooling at room temperature...
after, 50mL of H2O were added and then sucked off with a pipette, 4 times.... but nothing happens, except reforming of 2 layers... (no photo sorry)
after, i have separate the 2 layers, and put 50ml of isopropanol in the orange one
and i put it in the freezer... (actually 11h)
to be continued...
Last edited:
- Language
- 🇺🇸
- Joined
- Nov 5, 2024
- Messages
- 3
- Reaction score
- 1
- Points
- 3