Is there a way to synthesize 3-Chloropropiophenone · 3CMC?

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After one kilogram of bromination, I got 1.4 kilograms of product methylamine, 1500 ml toluene, 3000 ml. The final product that came out after acidifying PH6 was very little, only 40%, and the water was very dirty and black. I don’t know what went wrong.
 

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What I want to ask about is 4cmc. The word above is misspelled.
 

G.Patton

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Hi. Can you clearly explain what happened and what you need? It's completely unreadable.
 

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我需要2b4c合成4cmc的技術 我是台灣人我不太懂英文
 

G.Patton

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Hello, everything you need for successful synthesis is available on BB Forum. If you are not able to read, nobody can help.
 
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