Question how to feed p2np in a batch reactor ??

[tucoXxX]

hello gentlemen, how can I feed p2np into the reactor? there is a 2000ml dispenser but it gets clogged. need to be unlocked ?? if so, with what? as far as I know, the reactor cannot be dismantled during work.

 

[41Dxflatline]

Clogged with what?

 

[UWe9o12jkied91d]

He was trying to use the liquid addition funnel to add p2np.

 

[41Dxflatline]

I'm assuming he's dissolved it in IPA or methanol though?

 

[UWe9o12jkied91d]

Nope, it’s sorted now however

 

[tucoXxX]

managed to dose p2np . I simply poured it in several parts through an opening. I'm trying to vaporize IPA now. I'm at 80 degrees but it's not steaming. I use rotovap without vacuum. anyone have an idea?

 

[41Dxflatline]

I'm pretty sure you're not in a pocket universe that doesn't obey the laws of physics so you're not at 80C or you need glasses.

 

[tucoXxX]

I use a gentle vacuum. it does not suck the alcohol towards the condenser. what evaporates flows back. maybe a stronger vacuum is needed?