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High yielding 4MMC synthesis / 2B4MP

freedum

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What guide did you follow?
Care to post a step by step. Looks good. Congrats.
 

DragonLabz

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DCM and adiffication in water with hcl
 

HeavenChem

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If he used acidification with water and DCM, then he separated water layer with 4-MMC*HCl and then washed this layer with DCM multiple times. After that you can leave it in container for crystallization. Just my thoughts. Can be different from his method.
I think this is pretty good. This way is mostly used in MDMA synthesis, but can be used with mephedrone.
 

PharmacopeiaLabs

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did you apply heat? And if yes, time of applied heat after addition of methylamine?
 
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