Question Failed 2b4mp synthesis

[ifeelsorry]

So this my 4th time synthesing 2b4mp from 4 Methylpropiophenone

But this time i didn't get any type of 2b4mp instead i got this gluie stuff in jar

I put 150 ml 4 Methylpropiophenone in flask then added 120 ml Hbr and then slowly added peroxide 50% slowly till it stopped changing colours, after that i added water in flask, but this time it didn't crystalize 2b4mp? Why is that ? What did i do wrong i tried the same thing last 3 time and it got crystalaz? What can i do now? Is this stuff useless now? Should i throw it away or i can still make 2b4mp with this?

 

[ifeelsorry]

@WillD @Marvin "Popcorn" Sutton @freedum please check

 

[ifeelsorry]

@G.Patton @GhostChemist @$!$ please check

 

[ifeelsorry]

@The-Hive @Dr. MMX PLEASE CHECK

 

[WillD]

Write in detail how you synthesized it. Leave what you got in a cool place under a lid. Write the reagents and the amount of reagents that you used.

 

[ifeelsorry]

Okay so I will go in detail

I've peroxide 50% so when i first time synthesis i water water down it to 36%
But when i did 2nd and 3rd time synthesis i forgot it to water it down to 36% and i got better results i don't know how with peroxide 50%

So 4th time again i go with peroxide 50% but this time it didn't crystalize

This is what i followed ->

I added 150ml 4 Methylpropiophenone in flask, then added 120ml Hbr 48%
And mixed it for 10 minutes

Then i took 55ml peroxide 50% and added in dropping funnel and added dropwise slowly slowly, it was white when i added peroxide it became red orange then it again became white, i added till it stopped changing colour, i used around 30-35ml peroxide and temperature was between 40-50 mostly below 45 ( one more thing my thermometer doesn't touch the liquid stuff it stays 2-3 Inch above solution, that temperature I'm telling you)

After adding Peroxide i mixed it for 10more minutes then added 370ml water (normal okay okay cold water, not so chilled) after this stage it always crystallizat to some type of white gluie stuff, but this time it didn't there is something in gluie stuff is in liquid but its orange, so i leaved the mixture aside its been more than 24 hours

 

[ifeelsorry]

So now i don't know should i add more peroxide? Or one guy told ke adjust ph level (i don't know how to do that)? And somebody also told me that crystallizan is not necessary i can synthesis with liquid as well but again I dont know how to do that, it would be awesome if you could help me

 

[ifeelsorry]

When i start earning some money i will contribute some donation as thankyou gesture to maintain this forum

 

[WillD]

No need to add water after peroxide. Now leave on the stirring what you did. Perhaps measure pH as written above to solve whether it is necessary to add another HBr

 

[ifeelsorry]

https://bbgate.com/en-gb/threads/pr...ursor-for-mephedrone-two-different-ways.7042/

I added water because its mentioned in this synthesis, and it worked last 2 times, like after adding water it used to crystal in 10 minutes

 

[WillD]

If the reaction has not passed, water reduced concentration. You need to try to mix longer, can add heating up to 30*C.

 

[ifeelsorry]

How do i reduce water from solution because its already mix in it, there is layers tho in solution but I'm not sure which one should i remove and how, and if i add heating won't it burn 2b4mp? Because I've heard 2b4mp effect increase in heat

 

[ifeelsorry]

I should remove all the upper layer ? Leave the orange gluie stuff in it

 

[ifeelsorry]

Thanks man,bBut i already added peroxide should i remove water then add more peroxide? And stirrer?

 

[ifeelsorry]

So now i just turn on the stirrer and leave it? For how long? And what ph level do i need? How much hbr should i add ? Should i also turn in the stirrer with water because its already in it or should i try to filter out the water? Sorry for too many questions sir, I'm newbie to all this

 

[G.Patton]

First of all, are you sure that you've used 4'-methylpropiophenone?
There is clear video tutorial. Just repeat step by step.

Download Video

2-Bromo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

• Novator
• Aug 3, 2022
• 16
• 2-bromo-1-p-tolyl-propan-1-one 4-methylpropiophenone 4-mmc bromination cas 1451-82-7 cas 5337-93-9 mephedrone mephedrone hydrochloride mephedrone video synthesis

2-Bromo-4'-methylpropiophenone synthesis (CAS 1451-82-7) from 4'-methylpropiophenone with...

 

[ifeelsorry]

Yes it was 4 Methylpropiophenone, i made 2b4mp 3 time with same chemical, i don't know what i did wrong this time

I followed this method

https:// bbgate.com/en-gb/threads/pr...ursor-for-mephedrone-two-different-ways.7042/

 

[ifeelsorry]

How long do i need to stirrer it for after adding Peroxide? And the stuff I've now is it useless?? Should i throw it away? I think it can be recovered but i don't know how

 

[ifeelsorry]

What should i do now? Should i throw it away? The liquid i have ? @$!$ ?

 

[ifeelsorry]

How i fix it?

 

[ifeelsorry]

 

[ifeelsorry]

This video and the step i followed are same, but i added water after adding Peroxide, and he stirrer it till that liquid became powder and then added water, so next time how long should i stirrer it for???