Question Dmt freebase

[jennycraig]

Mimosa hostilis extraction, after got scraping from naaptha extraction, put dmt scraping in heptane (how muc?) and put on magnetic hotplate stirrer (50°C?), then draw up turkey baster put on pyrex put in freezer 12hrs. (then if want freebase as final product not fumaerate, how to extract dmt freebase from Heptane? Only wash in heptane 1ce, or 3 x like with naaptha?).
Thanks!

 

[darkwing]

I would recommend Naaptha, this means basicly dissolving an amount of freebase DMT in a minimal amount of
Naaptha, followed by the recovery of the DMT by freeze precipitation. The key to the
purification is to use the least amount of Naaptha necessary to dissolve the DMT, which is
typically 30-40mL per gram. When dissolving the DMT, you will notice that an insoluble
colored oil will remain at the bottom. This is the impurity you are going to want to remove. The Naaptha will dissolve little to none of this oil and after recovery of the DMT, you will see that it is significantly whiter. This process can be
repeated several times in order to further purify the product.

 

[darkwing]

Measure the desired amount of freebase DMT you wish to recrystallize

1 gram is used as an example, just multiply the Naaptha by the amount of grams.
The DMT is placed into a glass or other suitable container.
Now measure the amount of Naaptha needed to just dissolve the DMT
Remember, 30-40mL per 1 gram!
Pour the Naaptha into the glass containing the DMT and sit it in a bowl of boiling water
This setup acts as a hot water bath Let it sit for a few minutes and then work the DMT into the Naaptha. If the water cools too much, replace it with freshly boiled water and continue. Do your best to dissolve as much of the DMT as possible and you will notice an oily impurity on the bottom of the glass which will not dissolve This is what will be removed in order to purify the product. This oily impurity is mostly DMT-N-Oxide. Pour ONLY the Shellite into a fresh container Be very careful not to let any of the oily impurity come across into the new container as this is exactly what you are trying to remove!

 

[darkwing]

Cover the container and let it sit at room temperature for two to three hours, then place it in a refrigerator for a few hours, then in the freezer for +48 hours. The slow cooling of the Naaptha will result in a slower precipitation and hence combining of the DMT. This further helps to produce a purer product. after 48 hours put the container upside down for 10 minutes to remove as much of the Naaptha as possible. The recrystallized product is then fan dried for 30 minutes and collected. You will notice a drop in the weight of the DMT. This is because something has been removed. The more impure the DMT was, the less it will weigh after recrystallisation. Good luck!

 

[jennycraig]

Right on. Q: I already have the heptane, will do naaptha extraction as described above first, already have naaptha also. After naaptha, would like to do extraction with heptane for max purity. Know how to do heptane extraction but don't know how to get freebase dmt out of heptane after. Please advise asap. Thanks bros

 

[darkwing]

freebase DMT is made in the caustic soda conversion after the acid boil. Are you familiar with this method or need more advice?

 

[jennycraig]

The dmt workshop recipe right? Doing that initially, plan to switch to similar method mod has posted here, but wanting to do another purification with heptane, as described in workshop, unless everyone thinks totally unnecessary (?), don't want to make fumerate, just purify product by first naaptha pulls, then a heptane pull. Thoughts? If so, need to know how to extract dmt freebas3 from heptane solution afterwards, without going forward with making into fumerate? And what increase in purity should I have, after naaptha? After heptane? Thanks

 

[jennycraig]

Need more advice, first timer. Think I have it, not doing heptane pull, gotcha. Please help. Thanks