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- Jan 12, 2023
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With this mixture can I change from Benzaldehyde to Piperonal to create Pmk glycidate?
Reagents:
- Dimethylformamide 900 ml;
- Benzaldehyde 300 ml;
- Ethyl 2-chloropropionate 540 g;
- Benzyltriethylammonium chloride (TEBAC) 32 g;
- Potassium carbonate 780 g;
- Sodium hydroxide (NaOH) 135 g;
- Distilled water ~1.9 L;
- Concentrated (37%) aqueous hydrochloric acid (HCl) ~250 mL;