Aluminum amalgam with mercury nitrate monohydrate

[Barterpayne]

I have tried amalgamatiom with :

12 grams aluminum foil
0,3 grams mercury nitrate monohydrate
1 liter cold water in 2 liter round flask

Nothing is happening since 2 hour of vigorously shaking

Please help

 

[HIGGS BOSSON]

Perhaps you have bad foil, try to replace it. Mercury amalgam is always triggered in the presence of mercury salts and aluminum.

 

[Barterpayne]

I found out the issue .
A scammer sold le another compound that I trust it was Mercury nitrate Monohydrate, buy it was just crystalline white powder that has nothing to do with Mercury nitrate.
I am now stuck with :

My P2NP , My glacial acetic acid , IPA , Phosphoric acid , Acetone, caustic soda ( Sodium Hydroxide) and my Aluminum Foil is ok and premium one .
As I am in West Africa I don't know where to provide any Real Mercuric (II) Nitrate
And in my country mercury Hg and nitric acid .
I hope someone on bbgate could make me a give away of just 9 grams of that mercury nitrate I can start my business.
HIGGS help out

 

[HIGGS BOSSON]

If you have access to mercury thermometers, then finding nitric acid shouldn't be a problem. The synthesis of mercury nitrate production is easy.

 

[Barterpayne]

I am in a country where government have prohibited mercury , Lol . Because people use it in order to manufacture fake notes .
I have been in all pharmacy, none of them thermometer contains mercury .
And even if I find Mercury there is no way to find nitric acid . As yesterday I have been in my car around all chemical reseller .
So I try to find a deal with someone here to find a tiny quantity of Mercury nitrate directly.

 

[Care24hours@]

Can I get P2NP, I am from India and I am not able to get it in India? HIGGS help

 

[Barterpayne]

Mister care 24 hours
I have a deal with you . Here is the deal
You provide me Mercury (II ) Nitrate which is available in India .
And I can provide you p2np . I have 1 kg p2n In stock , and I can provide you 100 grams of my p2np
But I need just 15 grams of mercury nitrate which is available in India .
I can ship you from my town in West Africa !
Try to find a reliable quality ( not fake Mercury nitrate )

 

[Barterpayne]

Here is my p2np in my labs . I can send you 100 grams do you will have a good yield of 70 grams of amphetamine if you know how to synthesize well and have good equipment.
I will use DHL , and I will change the name of the chemical with DHL .
I will tell and declare them that this is Polyester resin Coating, so you wong get any issue with customs of India there ! I will declare low value . You will be able to get it in 3 to 6 days if you agree and if I ship before 24 décembre .

 

[Care24hours@]

Check and tell me if this is what you want?

 

[Barterpayne]

This is exactly the reagent we need

 

[Care24hours@]

Because I am new to all this and I haven't made anything yet. So I am asking you to make it. I don't have much idea. Please check and tell me.

 

[Barterpayne]

Buy with NUMEX Chemical India , their brand seems good !
I have just seen them online , and they really seems to be legit and reliable .

 

[Barterpayne]

I have successfully find elemental mercury contained in thermometer, and I buy to a local store nitric acid . Some one previously sold me fake Mercuric Nitrate .

Now after many attempt, I have been able to get 3,5 grams of amphetamine phosphate dried .
Yield is 35% for my first successful synthesis .

I will try to optimize parameter and input in order to yield 70% next attempt .

 

[G.Patton]

Nice, how much grams is your yield and how much p2np have you load there?

 

[Barterpayne]

My first tiled id 35% from 10 grams p2np .
So 3,5 grams dried amphetamine

 

[G.Patton]

It's not 35% yield. It it's 15.5% yield of amphetamine sulphate. Moles, grams, litres and chemical calculations

 

[Barterpayne]

Please respond mister Patton

 

[Barterpayne]

I use phosphoric acid .

 

[Barterpayne]

I don't know the calculation .
So how much is the resulting 70% yield of dried amphetamine phosphate from 100 grams of p2np ?

I mean when we have 100 grams of p2np , and we assume we will yield 70% of amphetamine, how much dried product we have in grams after synthesis

 

[G.Patton]

I've linked the topic, where you can find how to calculate it.

100g of p2np is 0.61 moles
In accordance with chemical reaction, you'll get same molar ratio of amphetamine phosphate.
0.61 moles * 233.2 = 142.9 g is theoretical yield you can get.
In practice ~70-80% is okay. It's 100-114g.