Question 3-CMC Synthesis (around 100g)

[salamanco]

Hi everyone,
This is my very first post here. I noticed this is not a toxic forum and people can really ask! So I'm trying to make some 3-CMC at home, and I got some products.
I saw 3 or 4 different methods and, as I'm new in this area, I wanted to ask you if the products I have are the proper ones.

(My level of experience = making really good homemade poppers)

- 1kg methylamine hcl
- 1l DCM
- 1kg Benzoyl-l-tartaric acid
- 500g NaOH
- 25l HCl 33%
- 2l Isopropylic Alc
- 1l ethyl acetate

Am I missing any chemicals?

Thank you guys! Have a nice week!

 

[HerrHaber]

Well the meta chlorinated propiophenone with or without halogen on the C2 (and the halogenating agent) is somewhat like attempting to bake bread without flour. You forgot the main ingredient.

 

[salamanco]

Totally forgot about it! I'm starting today and posting the results. Thanks

 

[Jackson]

you posted nothing

 

[1019er]

Seems to be an easy recipe! If it works.
Will try this soon.
I'm not sure if there is a big demand for this substance, so maybe 4mmc is.more lucrative!
Greez

 

[Jackson]

there is. 3cmc is verry good. like 4mmc but without the cat piss smell

 

[TryHard4Ever]

When you have the final product let me know, and in the mean time do you think it is posible to give a tutorial about home made poppers ?

 

[Berlin777]

I’m not an expert but I think it’s worth asking one of them if NaOH and DCM proportions are right

 

[Enrique13061991]

More dcm

 

[Dr. MMX]

why no 35-38% HCL instead of 33?

 

[$!$]

HCl can use 30% and is no problem

 

[G.Patton]

Hello, you won't get 3-CMC from this. You need 3'-Chloro-2-bromopropiophenone for that. Also, you can follow this method from Methamination step, just substitute precursor and recount reagents in the same molar ratio.

 

[Enrique13061991]

2bromo3chloroprof… is good too

 

[$!$]

Only on 3cmc