Acetophenone makes 1-phenyl-2-propanone (P2P)
Material:
Acetophenone (C6H5COCH3): 50 mL
Methyl iodide (CH3I): 30 mL
Potassium hydroxide (KOH): 10 g
Ethanol or dimethyl sulfoxide (DMSO): 100 mL
Steps and possible situations:
Alkaline treatment:
Operation: Dissolve 50 mL acetophenone in 100 mL...
Hello,
I just found out about this pretty new precursor of P2P:
Methyl 2-phenylacetoacetate CAS: 16648-44-5.
Can anyone help me to find the right synthesis to P2P with this precursor?
Thanks in advance.
Greetings,
MisterAnonymous.
Reagents and materials:
145 ml of unrefined P2P obtained through the reduction of P2NP with borohydride
300-400 ml of a 10% aqueous solution of potassium carbonate
4 liters of distilled water
500 ml (100 g of sodium chloride) of a 20% aqueous solution of sodium chloride
1-liter, 2-liter, 500...