mdp2np

  1. xoxo2.0

    Successful MDA .HCl synthesis from piperonal (with good yields)

    Hey i was just looking around the threads and want to share my experience with this synthesis ( as i didn't find any report for this in moderate scale ) I HAVE DONE THIS PROCEDURE ABOUT 4 TIMES BY NOW AND WOULD LIKE TO SHARE SOME OF IT. EQUIPMENT USED 500ML FLAT BOTTOM FLASK 500mm ALLIHN...
  2. MDP2NP Synthesis. Stage 2, 3, 4.

    MDP2NP Synthesis. Stage 2, 3, 4.

    Full MDP2NP synthesis from natural piperine. Stage 2: piperonal qualitative test (aldehyde test). Stage 3: MDP2NP synthesis. Stage 4: recrystallization of MDP2NP.
  3. MDP2NP Synthesis. Stage 1: Piperonal Synthesis.

    MDP2NP Synthesis. Stage 1: Piperonal Synthesis.

    Full MDP2NP synthesis from natural piperine. Stage 1: piperonal synthesis.
  4. GhostChemist

    MDP2NP Full Synthesis From Natural Piperine

    Stage 1. Synthesis of Piperonal. Extraction of piperine from black pepper has been demonstrated previously. Starting reagents and materials 5 g recrystallized piperine 100 + 50 ml THF 10 g Potassium permanganate + 200-300 ml water 800-1000 ml DCM 50-100 g anhydrous sodium sulfate 25 ml EtOH...
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