Amphetamin Synthesis from phenylpropanolamine hydrochloride with reduction using I2 and H3PO2.
Starting reagents and materials
4.84 g phenylpropanolamine hydrochloride
10.4 g I2
9.4 ml H3PO2
20-50 ml H2O
50 ml 25% NaOH (15-20 г NaOH)
3 g sodium thiosulfate
250-300 ml DCM
30-50 g Na2SO4...
Heyo! How do u extract iodine from an 11% povidone-iodine solution?
I followed the guide for extracting iodine from an alcohol solution using a polyethylene plate and water but that didnt really work out.
I do have some sodium hydroxide but i sadly dont have any hcl acid, nor any hydrogen...
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I've read articles where hypophosphorous has been been used in Microwave irradiation, iodine too being used in Microwave environment so I was wondering does anyone have any information on a Microwave irradiation of a Birch Reduction using hypo, Iodine and Psuedoephadrine?
Theoretically I...