hydrazine
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Wolff-Kishner reduction, large scale, feasible or just suicide?
As per title: I was trying to come up with a stereo-selective synthesis, but I'm stuck at one point where I have to remove a carbonyl. Turning it into an alcohol would vanish the selectivity goal. Now, wherever I look for information it's just people warning about preferring any other way is...- victorplum
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- carbonyl clemmensen hazard hydrazine large scale reduction wolff-kishner
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- Forum: Other
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How can i make Anhydrous Hydrazine?
Hello, I want make lsd with this method: Add 1.2 g of ergotamine hydrochloride to 4 ml of anhydrous hydrazine and heat 1 hour at 90°. Add 20 ml of water and evaporate in vacuo, to get d-iso-lysergic acid hydrazine. 1 g of the lysergic hydrazine is powdered well and added to 40 ml of 0.1 N (ice...