chloroform
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Chloroform synthesis help, to distill or not distill?
Hi, I looked up the synthesis of chloroform and managed to do it 2 times already using liquid bleach and acetone. But some places state that it should also be distilled after filtering if it was going to be used for humans. My problem is no one states the reason why it should be distilled. Is...- AcidBase
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- acid-base extraction chloroform clean distillation heroin
- Replies: 2
- Forum: Problems and Solutions
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Can I get some eyes on these crystals?
Whats this look like to you? I did a couple things. I heated ammonium chloride and formaldehyde with an alihn condenser and 110° turndown vacuum fitting on top and vacuum pump for a few hours and let it cool and filtered it. Then I distilled the liquid under vacuum for a couple hours and...- Osmosis Vanderwaal
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- 4-mmc ethyl acetate chloroform methanol methylamine hcl synthesis
- Replies: 9
- Forum: Laboratory FAQ
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Methiopropamine synthesis
Chloroform can react with chlorine gas and iron powder to form carbon tetrachloride and forms hydrogen chloride as a byproduct. Thiophene is brominated to 2-Bromothiophene with bromine in Carbon Tetrachloride. 2-Bromothiophene can react with ethyl acetoacetate and sodium ethoxide and using...- BlueDex
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- 1-(2-thiophenyl)-2-propanone bromination carbon tetrachloride chloroform copper (i) iodide enolate methylamine reductive amination
- Replies: 2
- Forum: Amphetamines (Phenylethylamines)