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Fastest way to synthesize 4mmc?
- Thread starter dodobird
- Start date
You do need a bout a day for it.
The 4mmc the fastest way can be obtained by nmp + dcm reaction (20min reaction), cooling down several minutes, washing about 30-60min, then acidificaction with hbr + water. Salt is already obtainted at 1c temp (ice bath)
Product is filtered and purified by crystalisation. First batch of Crystals can be obtained within 3-5h since the start.
The 4mmc the fastest way can be obtained by nmp + dcm reaction (20min reaction), cooling down several minutes, washing about 30-60min, then acidificaction with hbr + water. Salt is already obtainted at 1c temp (ice bath)
Product is filtered and purified by crystalisation. First batch of Crystals can be obtained within 3-5h since the start.