Question My shake and bake results with photos

[marges]

Merhaba

Birkaç kez çalkalayıp fırınladım ve uzun süre süzmeye bıraktığım tozları kuruttuktan sonra folyo üzerinde denedim ve kristalleşmedi. Folyo üzerinde siyaha dönüyor, resimlerde görüldüğü gibi duman neredeyse hiç çıkmıyor. Sizce nerede hata yaptım? Yoksa devam etmem mi gerekiyor?

 

[marges]

Hello

I did shake and bake a few times and after drying the powders that I had left to filter for a long time, I tried it on a foil and it did not crystallize. It turns black on the foil, as seen in the pictures, the smoke almost never comes out. Where do you think I made a mistake? Or do I need to continue?

 

[Osmosis Vanderwaal]

Shake and bake is broadly a style of manufacturing, it can be done with se Era chemicals and even reactions. We need to know what you did to even guess. You said should I finish it? It could very well be a bunch of starch from pills if you didn't extract them, that has soaked up freebase meth which is yellow and oily and dries very slowly, ifnthat what it is, you have to extract the freebase from the junk and hcl it

 

[marges]

My shake and bake experiments

Hello everyone, I am writing from Turkey, I came without watching Breaking Bad 😁 I have been following the forum for a long time. The more you look at it, the more complicated it becomes. I try to understand and produce by putting it into practice. I understand as I try 😁 Today I tried making a...

bbgate.com

I followed the steps here. I gassed the hcl and sodium salt in liquid form, but it did not snow. Do I need to put this powder in a container, add some hcl and dry it?

 

[marges]

Or do I need to add hcl and filter again?

 

[Osmosis Vanderwaal]

If it's got methanol in it, meth is freely solube in methanol and that would be why it doesn't precipitate

 

[Idrinkanhydrousammonia]

Definitely shouldve purified the ephedrine 3 cold acetone washes and a 99% isopropyl alcohol recrystallization would be perfect

 

[marges]

So, what is the reason why the resulting powder is yellow and oily? Is it because the cold medicine I use is dirty?

 

[Idrinkanhydrousammonia]

Seems to be soaked in solvent or freebase

 

[Idrinkanhydrousammonia]

https://bbgate.com/en/threads/shake-and-bake-remastered.13240/