Question SYNTHESIS MDA FROM HELIONAL HELP

kamikaze3030

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Hello friends. Can someone help me with this synthesis? In the image is the route used in the lab of the video that I left the link.

Laboratory video :

Used products:
Helional
Hydroxylamine
DMSO
trichloroethylene
sodium hydroxide hydrogen
peroxide
Isopropanol
hydrochloric acid
Baking soda
TCCA
 

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psy

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The video could literally show any synthesis. Without seeing chemicals it is difficult to tell what it going on. I am not Sherlock Holmes unfortunately. If the lab used the chemicals you mentioned, then yes, it is very likely it was done that way.
The video is extremely impressive, other than the fact that it got busted. 🤣
I have never seen a beckmann rearrangement for helional before. I figured it was getting oxidized to the carboxylic acid and then reacted with urea to form the amide.
Sorry I am not much help to your question, but thanks for sharing the video.
 
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