Hi Napoleon,
I found this:
Ephedrine Sulphate Injection Dosage and Administration
General Dosage and Administration Instructions
Ephedrine sulfate injection, 50 mg/mL must be diluted before administration as an intravenous bolus to achieve the desired concentration. Dilute with normal saline or 5% dextrose in water.....
How much (cc) did you use? If it was like the above, you were only getting about 1/20 of what you needed for the reaction.
Like what has been said by others, pour the liquid in a shallow, flat-bottomed dish or plate and allow all the water to evaporate. Scrape up the remaining residue and weigh it. This will be the ephedrine SALT. The MW of this will be the basis for calculating the amounts of the other reactants.