Register

What's new Search Customizer

JavaScript is disabled. You are safe. However, not all site features work fully without JS. For example, you will not be able to watch our video tutorials.

Question Amfetamīna bāzes attīrīšana

Thread starter Mohammed_Lee
Start date Aug 22, 2023

Mohammed_Lee

Don't buy from me

Resident

Aug 22, 2023

#1

Sveiki,

vai ir kāds veids, kā destilēt amfetamīna bāzes šķīdinātājus bez rotavatora?

Visu to labāko,

Lee

Solution

Depending of the quantity and nature of solvent, if in lower amount than the base and if your solvent have a low boiling point or if it is - under 90°C and non polar - you can just strip it under your hardest vacuum keeping your flask in gentle water bath. 30-40°C. Better to use a water pump for that or have a washing flask to keep your pump free of solvent. I bet you are talking about IPA, if it is you can simply dry it and acidify to get the salt and perform a recryst, if you really want If as oil you can simply do a vacuum distillation of the two products with eventually a short Vigreux.

Best Regards,

Captain Sandoz

Sort by date Sort by votes

CaptainSandoz

Don't buy from me

Resident

24 Aug

#2

Atkarībā no šķīdinātāja daudzuma un veida, ja tas ir mazākā daudzumā nekā bāze un ja jūsu šķīdinātājam ir zems viršanas punkts vai ja tas ir - zem 90 °C un nepolārs - jūs varat to vienkārši atdalīt zem vissmagākā vakuuma, turot kolbu maigā ūdens vannā. 30-40°C. Tam labāk izmantot ūdens sūkni vai mazgāšanas kolbu, lai sūknis būtu brīvs no šķīdinātāja. Ja runa ir par IPA, tad to var vienkārši izžāvēt un paskābināt, lai iegūtu sāli, un veikt rekristalizāciju, ja patiešām vēlaties, lai to izmantotu kā eļļu, varat vienkārši veikt abu produktu vakuumdestilāciju, beigās izmantojot īsu Vigreux metodi.

Ar vislabākajiem sveicieniem,

Captain Sandoz

Upvote 1 Downvote

Solution

Mohammed_Lee

Don't buy from me

Resident

25 Aug

#3

Paldies par garo atbildi!

Upvote 0 Downvote

You must log in or register to reply here.

Share:

Facebook Twitter Reddit Pinterest Tumblr WhatsApp Link

Top