3mmc sythese

Studenttt

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Tere,
Olen teinud 3 mmc valge Sythese video, reaktsioon on ka sama ja kõik läks hästi. Olen teinud kena välimusega kristallid, kuid efekt ei ole hea, ma arvan, et see on 2-bromo-3-metüülpropiofenooni Hiina.
Kas keegi on teinud 3 mmc või oli see probleem võib mind aidata
 

Didi

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On lihtne teha sama nagu 4mmc
 

Didi

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U tehtud viga sünteiss on lihtne tye sama kui u tehtud 4mmc u saab teha viga ja u saada madala pulbri mõju
 

WhalterWhite

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sõber püüdis teha sama sünteesi nagu 4cmc, kuid nüüd 2bromo 3 chloro. Esmalt tuli freebase tumepunane, 2bromo 4 chloro puhul on helekuldne kuldne. Siis pärast hapestamist muutus HCL mustaks. Kas keegi teab miks? Ph 5-6
 

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WhalterWhite

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Pärast 10 min.
 

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little-flower

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tere"" kas kellelgi on 2bromo3metüülpropiofenooni sulamistemperatuur?
 

ymaaah

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48°C sild
 

ymaaah

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nope 2bromo4metüülpropiofenooni puhul on 75°C, 2B3MP puhul 48°C bro ;D
 

little-flower

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ok" aitäh"" oled sa kindel,,ma ei leia kuskilt teavet sulamistemperatuuri kohta.
 
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ymaaah

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no problem dude :)
 
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