What the best road to crystalization 3cmc ?

dark_side_of_chemistry

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want to crystallize 3cmc. which solvent is best to use for the freezer method. I understand that I dissolve 1g 3cmc in 1 ml of water .. I understand that 0.5 of the solvent is to be equal to how much the product will dissolve. e.g. for 1kg of 3cmc in 1l of water, 0.5l of solvent is added? what do you think about crystallization in dcm?
 
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