Question Preperation of 40% aqueous methylamine solution

reggiesaws

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Hi. Can someone please advise the best and safest way to prepare a 40% aqueous methylamine from methylamine HCL? What are the safety precautions when doing this.
 

Mr.Blanks00

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how to make it by adding a concentrated solution of naoh in methylamine hcl and heating slowly to a temperature of 60% and the steam is run with a hose in a cold water solution.
 

T0lek511

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Just add NaOH and the methylamine gas keep bubbling trought distiled water and by weight and by volume you can find % of your solution. And if its higher then 40% just add water.
 

B APPLE

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May I ask how to make 40% methylamine water from methylamine hydrochloride, water, and sodium hydroxide
 
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