Question methylamin 40% solution in water

ossi

Don't buy from me
Resident
Joined
Sep 15, 2022
Messages
69
Reaction score
29
Points
18
hello,

I need help please. I need methylamine hydrochloride, but have only methylamin 40% in water solution.
how can I remove water easily and safe?
thanks
 

Osmosis Vanderwaal

Moderator in US section
Resident
Joined
Jan 15, 2023
Messages
1,308
Solutions
4
Reaction score
883
Points
113
:unsure::unsure::unsure::unsure::unsure::unsure: I'm thinking you bubble hcl gas through it, making it much more durable lewis acid, then evaporate it
 

Ortist

Don't buy from me
Resident
Joined
Apr 29, 2023
Messages
89
Solutions
1
Reaction score
54
Points
18

From the question I suppose you don't have any chem glassware nor knowledge, so you can do this:

1. Buy muriatic acid (35% is ok)
2. Put your methylamine bottle in a fridge to cool it down (but not freeze!)
3. Mix your cold methylamine with muriatic acid (add acid by small portions)
4. Check pH. If it is 7 or higher -> go to the step 3
5. Once you reached pH 6 or lower: boil out excess water (gentle boiling)
 
Top