ADBB

Aaryan

Don't buy from me
Resident
Language
🇺🇸
Joined
Feb 28, 2022
Messages
5
Reaction score
6
Points
3
Most legit vendors are only selling the precursors now.
''ADBB Precursor" to be exact. Try checking with your previous suppliers if they are capable of making the precursor. I hope this info will be helpful to those looking for noids out there. My team is working on this currently and if theres any progress i will let all of you know with proof. good day

This is what you guys will need

1) ADBB precursor (main material)
2) Three auxiliary material:
DMF ( Cas: 68-12-2 )
Anhydrous Pottasium Carbonate ( Cas: 584-08-7)
Bromobutane ( Cas: 109-65-9 )

3) Tools:
Stainless Steel or Glass Reaction Bottle with stirring and heating function
PH Detector and disposable filter paper
Buchner Funnel;vaccum filtration kit;vacuum pump

*If you use 1kg main material one time,5L capacity is enough*
 

WillD

Expert
Joined
Jul 19, 2021
Messages
774
Reaction score
1,060
Points
93
Reagents necessary for the synthesis of the main reagent (for ADBB):

(S)-2-Amino-3,3-dimethylbutanamide hydrochloride cas: 75158-12-2 1.1eq
1H-indazole-3-carboxylic Acid 1eq
DMF cas: 68-12-2
(S)-2-amino-3,3-dimethylbutanoate hydrochloride cas: 63038-27-7 1.1 eq
HOBt*H2O cas: 123333-53-9 1.1eg
EDC*HCl cas: 25952-53-8 1,5eq
Et3N cas: 121-44-8 3,5eq
EtOAc cas: 141-78-6
MgSO4 cas: 7487-88-9
 

Basil587

Don't buy from me
New Member
Joined
Apr 13, 2022
Messages
2
Reaction score
0
Points
1
It’s a scam
 

woohoo

Don't buy from me
New Member
Joined
Apr 21, 2022
Messages
56
Reaction score
22
Points
8
I want to learn serious chemistry.
Why some cannabinoids require strong bases like sodium hydride, but this is just potassium carbonate?
What should i learn to understand this difference?
 

WillD

Expert
Joined
Jul 19, 2021
Messages
774
Reaction score
1,060
Points
93
The alkylation reaction proceeds under various conditions. Strong bases allow the reaction to proceed faster, but they can affect the ester or amide group. Then the route above may not work.
 

DavidDavison2021

Don't buy from me
Resident
Joined
Apr 11, 2022
Messages
25
Reaction score
7
Points
3
Did this work out? I have not heard anything good about it! its still in the air? I do see that they are sending kits but so do they work?
 

WillD

Expert
Joined
Jul 19, 2021
Messages
774
Reaction score
1,060
Points
93
Due to prohibitions in China, they can send flour, and not a real reagent.
 

Hatermade

Don't buy from me
New Member
Joined
Mar 4, 2022
Messages
58
Reaction score
17
Points
8
How about they sent me chalk, and rice flour
 

Hatermade

Don't buy from me
New Member
Joined
Mar 4, 2022
Messages
58
Reaction score
17
Points
8
I did synthesize5cl from a kit that turned out great
 

dirtred

Don't buy from me
New Member
Joined
Apr 14, 2023
Messages
9
Reaction score
4
Points
3
me to and adbb percursors are available just got to find
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,727
Solutions
3
Reaction score
2,886
Points
113
Deals
1
Can your post synthesis report in our forum ?
 

Jailhmp

Don't buy from me
New Member
Joined
May 21, 2022
Messages
4
Reaction score
3
Points
3
Can we try it out could pay you for some
 

Hatermade

Don't buy from me
New Member
Joined
Mar 4, 2022
Messages
58
Reaction score
17
Points
8
Yes no problem.
 

Hatermade

Don't buy from me
New Member
Joined
Mar 4, 2022
Messages
58
Reaction score
17
Points
8
They working for me.
 

xiluh

Don't buy from me
Resident
Language
🇺🇸
Joined
Dec 3, 2021
Messages
20
Reaction score
15
Points
3
Does the "ADBB Precursor" still have a little "high" if i smoke it? or do not feel anything?
How to
 

madmoney69

Don't buy from me
Resident
Language
🇬🇧
Joined
Jan 29, 2022
Messages
165
Reaction score
160
Points
43
Truth is this : 5CL kits work, ADBB kits dont ( I heard now they say that have new version of adbb kit which I not tried). I talk from experience
 

jeanbostan

Don't buy from me
New Member
Joined
May 27, 2022
Messages
1
Reaction score
1
Points
1
Also the adbb kit works . I did it and it turned out ok .
 

WillD

Expert
Joined
Jul 19, 2021
Messages
774
Reaction score
1,060
Points
93
Yes, this can have some effect, but weak.
 

orgasmatron

Don't buy from me
Resident
Language
🇺🇸
Joined
May 2, 2022
Messages
25
Reaction score
14
Points
3
This synth, in the ingredients list one can find L-tert-leucine (63038-27-7) and L-tert-leucinamide (75158-12-2). It is not clear to me which one ( or both) is to be used, or if this is an option given to the chemist. Is it reasonable to say that Adb-b would be a tert-leucinamide derivative and mdmb-4en-pinaca would be a terc-leucine one? The adb-pinaca procedure suggests using tert-leucinamide and simultaneously mdmb-4en-pinaca is pointed as being the adb-pinaca derivative + the fluoro at carbon 5 in a number of places, but if structures are reviewed, one can find this difference and I can't tell exactly how high of a relevance this issue has. Just to seal the confusion over some observation time is, at the 'in-more-detail synthesis' described on the mdmb-4en-pinaca thread either reagent is nowhere to be found. I'm convinced I'm missing something so I will ask away, where is it, or why is it not?
Thank you
 
Top