90%+ ∆9-THC With ND ∆8-THC | AlCl3 / Aluminum Chloride SOP

[cake]

Finally, he made this public after more than a year of research:

• 90%≥ ∆9-THC Yield Extremely Fast (~1hrs)
• ND ∆8-THC
• Much safer than TIBA.

 

[blosuetoday]

Can somebody upload it here?

 

[cake]

I'm re-uploading it but I need to find a host rq.

 

[cake]

In case you missed it mate I re-uploaded to Mega down below.

 

[magdagessler]

Any chance to check the video on youtube. It doesnt work to me or some more info about the synthesis
I've checked sth and as I know it shoud be used DCM, low (-5 to 0 Celc.degree) temp. required however the amount of AlCl3 is unknown to me. Any idea, helpfull tips

 

[cake]

3% AlCl3 : CBD by weight.... So if you're using 100g CBD, use 3g AlCl3.

 

[cake]

I prefer n-Heptanes to DCM... Slightly less yield but DCM is so volatile!

 

[cake]

Also the reaction can be run even at -20C but you'll again get slightly less yield than staying within the -7C to -3C range. Past 0C and you'll start to get D8 selectivity.

 

[cake]

Here's a re-upload for anyone who can't access the YouTube video:
90%+ ∆9-THC With ND ∆8-THC | AlCl3 / Aluminum Chloride SOP

 

[magdagessler]

Thank you Cake

 

[cake]

You're welcome.

 

[Vodafone111]

So basically Rxn will not occur if solvents or Rxn mixture is too dry ?
He mentioned mass production method using HCl aq and heptane with molecular sieves before.

It seems like Hydro Chlorine can isomerise CBD into D9 under inert atmosphere and shall be the best acid for D9 selectivity.
This time he chose Aluminium Chloride for less-moisture.

AlCl3 will form HCL gas when exposed to the moisture (H2O).
Slight amount of H2O is needed to perform this reaction because it cannot release or form HCL inside Rxn.

the same logic, you can bubble dry HCL gas into CBD isolate dissolved in heptane or DCM, dried by Calcium Chloride.

Correct me, if my understanding were wrong.

 

[William D.]

Synthesis in ethanol with a small percentage of hydrochloric acid, I think, will be more convenient

 

[grävling]

If you want high D9 no d8 then this is the.way to go.
Hcl in ethanol makes mostly D8 and a bunch.of nasty sideproducts

 

[William D.]

It depends on the conditions you can use. But in general, all conversion methods use acid and temperature, either together or separately. Success will depend on concentration and time. If you have analytical skills, you will have no problem with many methods.

 

[grävling]

If i would have acces analytical, i would defenitifly not be reading here....

 

[William D.]

We will make a method with Al chloride. I saw not the best results, but our team did not try this route. Soon I will let you know. I think to continue ultrasonic synthesis when cooling to obtain selective results, because purity is higher than in other methods. For Al chloride, I saw data about 70%, but I think that determined conditions for time, temperature and solvents can change productivity and purity.